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1 article(s) from Yurkovskaya, Alexandra V

Synthesis of nucleotide–amino acid conjugates designed for photo-CIDNP experiments by a phosphotriester approach

Tatyana V. Abramova,
Olga B. Morozova,
Vladimir N. Silnikov and
Alexandra V. Yurkovskaya

Beilstein J. Org. Chem. 2013, 9, 2898–2909, doi:10.3762/bjoc.9.326

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Figure 1: Model compounds for the TR NMR photo-CIDNP experiments: conjugates of 4-benzoylbenzoic acid, 2’-deo...

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Scheme 1: Synthesis of functionalized derivatives of 4-benzoylbenzoic acid (9), L-tryptophan (11, 16) and L-t...

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Scheme 2: Synthesis of conjugates 1–3: i) 2,4,6-triisopropylbenzenesulfonyl chloride (TPSCl), 1-methylimidazo...

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Scheme 3: Synthesis of conjugates 4 and 5: i) TPSCl, MeIm, Py; ii) AcOH/H₂O; iii) p-chlorophenyl dichlorophos...

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Scheme 4: Synthesis of conjugates 6–8. i) TPSCl, MeIm, Py; ii) TBAF in Py/H₂O, then NH₃/H₂O; iii) TBAF in Py/H...

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Published 18 Dec 2013

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